Used Lab Equipment

Features:

• Optimized for high-throughput applications and sub two micron column particles
• Maximum reproducibility with isothermal injection and separation
• Greater application flexibility with multiple sample formats
• Superior robustness with a diamond coated high pressure valve Accela Photo Diode Array Detector
• Highest detection sensitivity with proprietary LightPipe technology
• Designed for U-HPLC separations with a 1cm path length, 2µL LightPipe flowcell
• Maximum peak resolution with fiberoptic beam shaper
• Easy maintenance with integrated wavelength validation

Specifications:

• Sample capacity:
  • 200 vials in five removable trays
  • 288 samples in three 96-well microplates
  • 1152 samples in three 384-well microplates
• Standard vial:8 mL volume
• Injection precision: < 1.0% RSD at 5 μL and up
• Partial loop injection volume:
  • 10 μL with standard 25 μL sample loop and 250 μL syringe
  • Up to 1000 μL injection volume with optional loops and syringes
• Fixed loop (full loop) injection volume:
  • 25 μL with standard loop and 250 μL syringe
  • Up to 1000 μL injection volume with optional loops and syringes
• Sample carryover:
  • < 0.1%
  • 6 mL flush volumes, user-specified for internal and external needle wash cycles
• Minimum sample volume: 1 μL can be injected from 5 μL
• Needle height control:
  • Programmable in 0.1 mm increments
  • Active vial bottom search selectable on/off
• Column oven: Programmable in 1 °C increments from 5 to 95 °C
• Tray temperature control:
  • Programmable in 1 °C increments from 0 to 60 °C
  • Typical vial temperature from 4 to 50 °C
• Reagent vials: Four 16 mL vials can be specified for flush/wash or dilution functions
• Remote inputs: Pump ready, inject hold
• Remote outputs: Pump stop, autosampler ready, inject, gradient start, four timed events
• Ambient environment:10 to 40 °C, 5 to 95% relative humidity, non-condensing
• Power requirements: 100/120/220/240 Vac nominal; 50/60 Hz, 550 VA

Specifications:

• Injection range: From 0.1 – 100 µl in 0.1 µl increments
• Replicate injections: From 1 – 99 from one vial
• Injection cycle time: Typically 50 s, depending on draw speed and volume
• Sample capacity: 100 × 2 ml vials in tray

Specifications:

• Autosampler (Chiller Compatible)
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range: 1– 100 µl in 0.1 µl increments Up to 1500 µl with multiple draw (hardware modification required)
• Replicate injections: 1– 99 from one vial
• Precision:
  • Typically < 0.5 % RSD of peak areas from 5 – 100 µl
  • Typically < 1 % RSD of peak areas from 1 – 5 µl
• Minimum sample volume: 1 µl from 5 µl sample in 100 µl microvial, or 1 µl from 10 µl sample in 300 µl microvial
• Carryover: Typically < 0.1 %, < 0.05 % with external needle cleaning
• Sample viscosity range: 2 – 50 cp
• Replicate injections per vial: 1 – 99
• Sample capacity:
  • 100 × 2-ml vials in 1 tray
  • 40 × 2-ml vials in ½ tray
  • 15 × 6-ml vials in ½ tray (Agilent vials only)
• Injection cycle time: Typically 50 s depending on draw speed and injection volume

Can be sold as an individual component or as part of a complete stack

Specifications:

• Autosampler Thermostat
• Operating temp range: 4 to 40°C (39 to 104°F)
• Operating humidity range: < 95%, non-condensing
• Maximum Power Consumption [VA]: 260 VA
• Maximum Power Consumption [W]: 210 W
• BTU: 717

Can be sold as an individual component or as part of a complete stack

Specifications:

• Autosampler Thermostat
• Operating temp range: 4 to 40°C (39 to 104°F)
• Operating humidity range: < 95%, non-condensing
• Maximum Power Consumption [VA]: 260 VA
• Maximum Power Consumption [W]: 210 W
• BTU: 717

Can be sold as an individual component or as part of a complete stack

Specifications:

• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Communications Controller-area network (CAN). RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range:
  
  • – 8 µl in 0.01 µl increments with the small loop capillary
  • – 40 µl in 0.01 µl increments with the extended loop capillary
• Precision:
  • Typically < 0.5 % RSD of peak areas from 5 – 40 µl,
  • Typically < 1 % RSD from 1 – 5 µl
  • Typically < 3 % RSD from 0.2 – 1 µl
• Sample viscosity range: 2 – 5 cp
• Sample capacity:
  • 2× well-plates (MTP) + 10 × 2 ml vials
  • 100 x 2 ml in one tray
  • 40 x 2 ml in half tray
• Injection cycle time:
  • Typically, < 30 s using following standard conditions:
  • Default draw speed: 4 µl/min
  • Default eject speed: 10 µl/min
  • Injection volume: 0.1 µl
• Carry-over:
  • Typically < 0.05 % using the following conditions:
  • Column: 150 x 0.5 mm Hypersil ODS, 3 µm
  • Mobile phase: Water/Acetonitrile = 85/15
  • Column Flow rate: 13 µl/min
  • Injection volume: 1 µl caffeine (=25ng caffeine), 1 µl water to test carryover
  • Outside wash of needle before injection: 20 sec with water using flush port

Specifications:

• Sample capacity: 100 x 2 ml vials in 1 tray. Microvials (100 or 300 µl) with sleeves (reduced cooling performance with microvials)
• Settable injection volume
  • to 8 µl with small loop capillary
  • to 40 µl with extended loop capillary
• Precision
  • Typically < 0.5 % RSD from 5 to 40 µl
  • Typically < 1 % RSD from 1 to 5 µl
  • Typically < 3 % RSD from 0.2 to 1 µl
• Minimum sample volume: µl from 5 µl sample in 100 µl microvial, or 1 µl from 10 µl sample in 300 µl microvials
• Carryover
  • Typically < 0.1 % without automated needle wash
  • Typically < 0.05 % with external needle cleaning and 1 µl injection volume
• Sample viscosity range: 2 - 5 cp
• Recommended pH-range: - 8.5 solvent with pH < 2.3 should not contain acids which attack stainless steel. Upper pH range is limited by fused silica capillaries
• Material in contact with solvent: Stainless steel, sapphire, PTFE, PEEK, fused silica
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in aintenance areas, error detection and display
• Housing: All material recyclable

Can be sold as an individual component or as part of a complete stack

The Agilent 1100 Series Dual Loop Autosampler is a fixed loop sampler with two different sample loops. As a consequence of this design the metering device, also referred to as syringe, is not a part of the solvent flow path from pump to HPLC column. An additional flush solvent bottle is used to rinse this part of the hydraulic path after each injection. In order to minimize carryover, the sampler is equipped with a needle wash function which dips the needle into a wash vial or the wash port. The wash port is fed by a peristaltic pump and can be operated with most common HPLC solvents.

Specification:

• Weight: 14 kg (29.8 lbs)
• Dimensions (H x W x D): 200 x 345 x 440 mm (8 x 13.5 x 17 in.)
• Line voltage: 100 - 240 VAC, ±10 % (wide-ranging capability)
• Line frequency: 50 or 60 Hz, ±5 %
• Power consumption (apparent power): 200 VA
• Power consumption (active power): 180 W
• Ambient operating temperature:  4 - 55 °C (41 - 131 °F)
• Ambient non-operating temperature: -40 - 70 °C (-4 - 158 °F)
• Humidity: < 95 %, at 25 – 40 °C (77 – 104 °F) non condensing
• Operating altitude: up to 2000 meters (6500 ft)
• Non-operating temperature: top to 4600 meters (14950 ft)
• Safety standards (IEC, CSA, UL): Installation category II, pollution degree 2

Specifications:

• Pressure: Operating range 0 – 40 MPa (0 – 400 bar, 0 – 5800psi)
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range:
  • 900 µl in 0.1 µl increments (recommended 1 µl increments)
  • Up to 1800 µl with multiple draw (hardware modification required)
  • Up to 5000 µl with multiple draw (hardware modification required)
• Replicate injections: – 99 from one vial
• Precision:
  • Typically < 0.5% RSD of peak areas from 5 – 2000 µl,
  • Typically < 1% RSD of peak areas from 2000 – 5000 µl
  • Typically < 3% RSD of peak areas from 1 – 5 µl
• Minimum sample volume:
  • µl from 5 µl sample in 100 µl microvial
  • 1 µl from 10 µl sample in 300 µl microvial
• Sample viscosity range: 0.2 – 50 cp
• Sample capacity:
  • 100 × 2-ml vials in 1 tray
  • 15 × 6-ml vials in ½ tray (Agilent vials only)
• Injection cycle time: Typically 50 s, depending on draw speed and injection volume

The Agilent 1200 ALS Thermostat, G1330A controls temperature for either HPLCs or fraction collectors. The ALS thermostat contains Peltier-controlled heat exchangers. A fan draws air from the area above the sample vial tray of the autosampler and is then blown through the fins of the cooling/heating module. There it is cooled or heated according to the temperature setting.

Specifications:

• Weight: 20.7 kg (45.6 lbs)
• Dimensions: 140 × 345 × 435 mm (5.5 × 13.5 × 17 inches)
• Line Voltage: 100 – 120 or 220 – 240 VAC, ± 10 % Automatic selection
• Line Frequency: 50 or 60 Hz, ± 5 %
• Power consumption Autosampler: 300 VA 
• ALS Thermostat: 260 VA

Specifications:

• Pressure: Operating range 0 – 40 MPa (0 – 400 bar, 0 – 5800psi)
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range:
  • 900 µl in 0.1 µl increments (recommended 1 µl increments)
  • Up to 1800 µl with multiple draw (hardware modification required)
  • Up to 5000 µl with multiple draw (hardware modification required)
• Replicate injections: – 99 from one vial
• Precision:
  • Typically < 0.5% RSD of peak areas from 5 – 2000 µl,
  • Typically < 1% RSD of peak areas from 2000 – 5000 µl
  • Typically < 3% RSD of peak areas from 1 – 5 µl
• Minimum sample volume:
  • µl from 5 µl sample in 100 µl microvial
  • 1 µl from 10 µl sample in 300 µl microvial
• Sample viscosity range: 0.2 – 50 cp
• Sample capacity:
  • 100 × 2-ml vials in 1 tray
  • 15 × 6-ml vials in ½ tray (Agilent vials only)
• Injection cycle time: Typically 50 s, depending on draw speed and injection volume

Features:

The Agilent 1260 Infinity II Vialsampler is an autosampler designed for the reliability and ease-of-use needed for routine pharmaceutical tasks and quality control, as well as for environmental and food analyses. It can house optionally the integrated column compartment for two LC columns with temperature control up to 80 °C, as well as a sample thermostat for stable temperature control from 4 °C - 40 °C, all within one module.

Specifications:

• High capacity - up to 132 vials (2 mL) or up to 36 vials (6 mL).
• Reliable injections -  0.1 to 100 µL injections for up to 600 bar (G7129A) and up to 800 bar (G7129C).
• Easy volume extensions- for injection volumes up to 1,500 µL (G7129A), or up to 1,800 µL (G7129C) for applications ranging from microbore to semi-preparative chromatography.
• Lowest carryover - with an in needle flush port included, for rinsing the outside of the needle.
• Efficient temperature control - with an integrated column compartment as an option or upgrade available. Which holds two columns up to 30 cm length, and provides heating capacity from 5 degrees above ambient up to 80 °C for reproducible chromatography data at optimized resolution.
• Integrated sample thermostat- available as an option or upgrade, providing cooling and heating (with thermostat) in the range from  4 °C - 40 °C.
• Low internal volume - for minimum contribution to a system's total internal volume, which can be even further reduced using bypass mode.
• Increased productivity - with overlapped injections.
• Customizable injection program - available for customizing advanced injections as well as for sample preparation steps upfront injection.

Includes 1 year Service Contract, Installation, and a PM at 6 months

Includes:

• AB Sciex API4000 LC/MS/MS
• Enhanced high performance triple quadrupole mass spectrometer system
• Line transformers
• Turbo V Ion Source (with APCI and ESI probes)
• Roughing Pump
• Windows 7 Computer loaded w/ Analyst Software 1.6
• Cart
• Agilent 1100 HPLC and CTC Autosampler
  • G1322 Degasser
  • G1312A Binary Pump
  • G1316A Column Compartment
  • G1323A Game Boy
  • CTC Autosampler

• Monitor – Mouse – Keyboard
• Cables and Manuals

Specifications:

• Detector type: Pulse Counting CEM
• Dynamic Range: 5 orders of magnitude
• Ionization Sources: ESI, APCI
• Mass Accuracy / Stability: 0.1 Da over 8 hours, 0.15 Da over 24 hours
• Mass Range: 5-3,000
• Polarity Switching Time: 700 ms
• Scan Speed (Quad): 24,000 Da/sec
• Scan Types: Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM
• Sensitivity MRM Mode: 200 fg Reserpine on column: S/N > 1,200, C.V. < 5%

Innovative QJet ion guide technology dramatically improves sensitivity by capturing and focusing more ions generated by the efficient TURBO V ion source. And the TURBO V source virtually eliminates cross-contamination, even with high-concentration samples.  New innovations in sensitivity like QJet ion guide technology make it possible to reach the lowest limits of detection. Combining QJet ion guide technology with the proven TURBO V ion source and a powerful new generation of Analyst software results in a robust, high throughput platform ideal for all phases of pharmaceutical development.

Includes:

• AB Sciex API5000 LC/MS/MS
• Enhanced high performance triple quadrupole mass spectrometer system
• Line transformers
• Turbo V Ion Source (with APCI and ESI probes)
• Roughing Pump

• Windows 7 Computer loaded w/ Analyst Software 1.6

• Cart
• Agilent 1100 HPLC and CTC Autosampler
  • G1322 Degasser
  • G1312A Binary Pump
  • G1316A Column Compartment
  • G1323A Game Boy
  • CTC Autosampler

• Monitor – Mouse – Keyboard
• Cables and Manuals

Specifications:

• Detector type: Pulse-counting channel electron multiplier (CEM) detector
• Dynamic Range: 1 cps to 4 x 10(6) cps (pulse counting)
• Ionization Sources: ESI, APCI
• Mass Accuracy / Stability: 0.01% over the entire mass range
• Mass Range: 5 – 1250 m/z
• Scan Types:  Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM

The Leap technologies CTC PAL HTC Auto sampler for HPLCs offer Precise and Accurate sample Loading, high throughput, flexible analysis while taking up limited bench space.

Includes:

• HTC PAL Autosampler (Width: 534mm Depth: 385mm Height: 648mm)
• Temperature controlled sample storage 3 drawer
• XYZ injector/Arm
• LC Injection valve- 6 port
• Wash station
• Gameboy controller
• Power Supply
• Manual