Used Lab Equipment

Features:

• Extended flow rate range
• Without changing pump heads, provides flow rates up to 100 mL/min at 400 bar
• For preparative and analytical applications with low flow rates (0.5 mL/min, upward), provides precise high-pressure binary gradient formation with low delay volume (700 uL)
• Automated seal wash using a peristaltic pump extends seal lifetime
• Pumps stop in response to column blockage or leaks
• Automated electromagnetic purge valve simplifies system setup
• Software provides solvent level control that keeps the pump from running dry

Can be sold as an individual component or as part of a complete stack

Includes: 

• Qty (2) - G1361A Agilent 1100 Series Prep Pumps
• G1315A DAD Diode Array Detector (G1314A VWD Detector also available)
• G2258A Agilent 1100 Prep Autosampler
• G1364B AFC Automated Fraction Collector
• Computer Loaded with ChemStation
• Monitor – Mouse – Keyboard
• Cables and Manuals

Includes:

• Qty (2) - G1361A Agilent 1100 Series Prep Pumps
• G1315A DAD Diode Array Detector (G1314A VWD Detector also available)
• G2258A Agilent 1100 Prep Dual Loop Autosampler (Manual Injector also an option)
• G1364B AFC Automated Fraction Collector
• Computer Loaded with ChemStation
• Monitor – Mouse – Keyboard
• Cables and Manuals

G1361 Prep Pump

Features:

• Extended flow rate range
• Without changing pump heads, provides flow rates up to 100 mL/min at 400 bar
• For preparative and analytical applications with low flow rates (0.5 mL/min, upward), provides precise high-pressure binary gradient formation with low delay volume (700 uL)
• Automated seal wash using a peristaltic pump extends seal lifetime
• Pumps stop in response to column blockage or leaks
• Automated electromagnetic purge valve simplifies system setup
• Software provides solvent level control that keeps the pump from running dry

Specifications:

• Pressure: Operating range 0 – 40 MPa (0 – 400 bar, 0 – 5800psi)
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range:
  • 900 µl in 0.1 µl increments (recommended 1 µl increments)
  • Up to 1800 µl with multiple draw (hardware modification required)
  • Up to 5000 µl with multiple draw (hardware modification required)
• Replicate injections: – 99 from one vial
• Precision:
  • Typically < 0.5% RSD of peak areas from 5 – 2000 µl,
  • Typically < 1% RSD of peak areas from 2000 – 5000 µl
  • Typically < 3% RSD of peak areas from 1 – 5 µl
• Minimum sample volume:
  • µl from 5 µl sample in 100 µl microvial
  • 1 µl from 10 µl sample in 300 µl microvial
• Sample viscosity range: 0.2 – 50 cp
• Sample capacity:
  • 100 × 2-ml vials in 1 tray
  • 15 × 6-ml vials in ½ tray (Agilent vials only)
• Injection cycle time: Typically 50 s, depending on draw speed and injection volume

Specifications:

• Pressure: Operating range 0 – 40 MPa (0 – 400 bar, 0 – 5800psi)
• GLP features: Early maintenance feedback (EMF), electronic records of maintenance and errors
• Communications: Controller-area network (CAN). GPIB (IEEE-448), RS232C, APG-remote standard, optional four external contact closures and BCD vial number output
• Safety features: Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display
• Injection range:
  • 900 µl in 0.1 µl increments (recommended 1 µl increments)
  • Up to 1800 µl with multiple draw (hardware modification required)
  • Up to 5000 µl with multiple draw (hardware modification required)
• Replicate injections: – 99 from one vial
• Precision:
  • Typically < 0.5% RSD of peak areas from 5 – 2000 µl,
  • Typically < 1% RSD of peak areas from 2000 – 5000 µl
  • Typically < 3% RSD of peak areas from 1 – 5 µl
• Minimum sample volume:
  • µl from 5 µl sample in 100 µl microvial
  • 1 µl from 10 µl sample in 300 µl microvial
• Sample viscosity range: 0.2 – 50 cp
• Sample capacity:
  • 100 × 2-ml vials in 1 tray
  • 15 × 6-ml vials in ½ tray (Agilent vials only)
• Injection cycle time: Typically 50 s, depending on draw speed and injection volume

Features:

The Optima MAX and MAX-E (see Figure 1-1) microprocessor controlled tabletop ultracentrifuges generate high centrifugal forces for a variety of high-speed applications. The instrument design features a variable-frequency induction drive, the thermoelectric temperature control system, self-purging vacuum system, rotor overspeed identification system, program memory that can contain up to ten five-step programs, and a choice of acceleration and deceleration rates.

Manual and programmed operation are available. • In manual operation, you enter the individual run parameters before beginning each run. • In programmed operation, you can duplicate runs quickly and accurately by selecting one of ten programs previously entered into the program memory. Each program can contain up to five steps. User messages and/or audible signals are provided to alert you to conditions that may need attention. An optional feature of the Optima MAX or MAX-E is the RS 232C Interface Accessory, which enables it to be connected to a personal computer. Information about this feature will be supplied upon request.

Specifications:

Only values with tolerances or limits are guaranteed data. Values without tolerances are informative data, without guarantee.

Speed

• Set speed:
• Optima MAX . . . . . . 5 000 to 130 000 rpm in 1 000-rpm increments
• Optima MAX-E . . . . 5 000 to 100 000 rpm in 1 000-rpm increments
• Speed control . . . . . . . . . . . . . actual rotor speed, ±50 rpm of set speed
• Speed display . . . . . . . . . . . . actual rotor speed in 100-rpm increments above 5 000 rpm and 10-rpm increments at speeds below 5 000 rpm

Time

• Set time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . to 99 hours 59 minutes
• Time display
• Manual operation . . . . . . . . . . . . . . . indicates run time remaining
• Programmed operation . . . . . . . . . . . . . . . . time remaining in step
• Temperature
• Set temperature . . . . . . . . . . . . . . . . . . . . 0 to 40°C in 0.1° increments
• Temperature control (after equilibration). . . . . ±2°C of set temperature
• Temperature display. . . . . . . . . . . . . . . . . . . . . actual rotor temperature in 0.1° increments
• Ambient temperature range . . . . . . . . . . . . . . . . . . . . . . . . . 15 to 35°C
• Humidity restrictions. . . . . . . . . . . . . . . . . . . . . . . . <95% (noncondensing)
• Vacuum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . below 10 microns (1.34 Pa)
• Acceleration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 acceleration profiles—9 slow rates from 0 to 5 000 rpm followed by full acceleration to set speed; or maximum acceleration
• Deceleration . . . . . . . . . . . . . . . . . 11 deceleration profiles—10 slow rates n from 5 000 to 0 rpm, including coasting to a stop without brake; or full dynamic braking from set speed
• Dimensions
• Width . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73.7 cm (29 in.)
• Depth . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58.4 cm (23 in.)
• Height. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58.4 cm (23 in.)
• Weight . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99 kg (217 lb)
• Ventilation clearances (sides and rear) . . . . . . . . . . . . . . . . 7.6 cm (3.0 in.)
• Finishes
• Control panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . coated polycarbonate
• Top surface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . urethane paint
• Other surfaces. . . . . . . . . . . . . . . . . . . . . . . . . . . . general purpose paint
• Electrical requirements
• 100-V instrument . . . . . . . . . . . . . . . . . . . 90–110 VAC, 12 A, 50/60 Hz
• 120-V instrument . . . . . . . . . . . . . . . . . . 100–130 VAC, 12 A, 50/60 Hz
• 220/240-V instrument . . . . . . . . . . . . . . . . . 198–254 VAC, 6 A, 50 Hz
• Maximum heat dissipation into room under
• steady-state conditions . . . . . . . . . . . . . . . . . . . . . . 1750 Btu/hr (0.5 kW)
• Noise level 0.91 m (3 ft) in front of centrifuge . . . . . . . . . . . . . . . . <60 dBa
• Installation category . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . II

Pollution degree. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Features:

The 600 pumps is quaternary, low-pressure mixing pumps with a built-in solvent degassing system and an automatic calibration feature.

Specifications:

• Flow rate range: 1 to 5000 μL/min
• Backpressure range: 0 to 600 bar (8702 psi)
• Residual pulsation: < 2 bar Amplitude
• Flow rate accuracy: ±0.5% or 1 μL/min, whichever is greater
• Gradient composition accuracy: ±0.5% absolute
• Gradient resolution: 1% from 0 to 100%
• Firmware version: (November 2010) 23.67 e
• Gradient composition range: 0 to 100% from up to 4 independent feed channels employing 2 of them at the same time
• Delay volume 90 μL (LDA): + 65 μL (static mixer)

The HP / Agilent 1100 HPLC series is the current model and arguably the best design in the industry because of the optimized design of the quaternary pump ensuring virtually pulse-free and stable solvent flow, with dual floating pistons in series, precisely servo-controlled. This design with variable stroke volume allows pulse-free solvent delivery and efficient mixing. An inlet-valve electronically activated and synchronized to piston stroke - eliminates vapor formation with volatile solvents and is maintenance free. With high-speed proportioning valve and pre-configured vacuum degasser, for convenient low-pressure mixing of up to four solvents and highest flexibility in solvent choices.

 Features:

• Ease-of-use - handheld control module lets you enter operating parameters fast, store methods easily and display pressure profile, diagnostics and task-oriented information.
• Durable - stainless steel, titanium, gold, ruby, sapphire, ceramics, PEEK and PTFE ensure long lifetime. Seal wash option for high salt mobile phases keeps maintenance to a minimum for lower operation costs.
• Wide flow range - up to 10 ml/min for broad HPLC work, including semi-preparative separations.
• Better for GLP - built-in leak and pressure test with graphical presentation of pressure profiles, and early maintenance feedback.

Specifications:

• Hydraulic system: Dual piston in series pump with proprietary servo-controlled variable stroke drive, floating pistons and active inlet valve
• Settable flow range: .001– 10 ml/min, in 0.001 ml/min increments
• Flow range: 2 – 10.0 ml/min
• Recommended pH range: – 12.5, solvents with pH > 2.3 should not contain acids which attack stainless steel.
• Operating voltage: 230V

The G1311A is an optimized design ensuring virtually pulse-free and stable solvent flow with dual floating pistions.  An inlet valve electronically activated and synchronized to piston stroke eliminates vapor formation with volatile solvents and is maintenance free.  Instrument comes equipped with four solvent inlets with built-in gradient control. 

Specifications:

• Configurable Flow Range: 0.001 – 10ml/min – in 0.001ml/min increments
• Flow Range: 0.2 – 10.0 ml/min
• Recommended pH Range: 1.0 – 12.5, solvents with pH > 2.3 should not contain acids which attack stainless steel
• Gradient Formation: Low pressure quaternary mixing/gradient capability using proprietary high-speed proportioning valve. Delay volume 800-1100µl, depending on back pressure

The G1311A is an optimized design ensuring virtually pulse-free and stable solvent flow with dual floating pistions.  An inlet valve electronically activated and synchronized to piston stroke eliminates vapor formation with volatile solvents and is maintenance free.  Instrument comes equipped with four solvent inlets with built-in gradient control. 

Specifications:

• Configurable Flow Range: 0.001 – 10ml/min – in 0.001ml/min increments
• Flow Range: 0.2 – 10.0 ml/min
• Recommended pH Range: 1.0 – 12.5, solvents with pH > 2.3 should not contain acids which attack stainless steel
• Gradient Formation: Low pressure quaternary mixing/gradient capability using proprietary high-speed proportioning valve. Delay volume 800-1100µl, depending on back pressure

The G1311A is an optimized design ensuring virtually pulse-free and stable solvent flow with dual floating pistions.  An inlet valve electronically activated and synchronized to piston stroke eliminates vapor formation with volatile solvents and is maintenance free.  Instrument comes equipped with four solvent inlets with built-in gradient control. 

Specifications:

• Configurable Flow Range: 0.001 – 10ml/min – in 0.001ml/min increments
• Flow Range: 0.2 – 10.0 ml/min
• Recommended pH Range: 1.0 – 12.5, solvents with pH > 2.3 should not contain acids which attack stainless steel
• Gradient Formation: Low pressure quaternary mixing/gradient capability using proprietary high-speed proportioning valve. Delay volume 800-1100µl, depending on back pressure

Specifications:

• Hydraulic system: Two dual piston in series pumps with proprietary servo-controlled variable stroke drive, floating piston design and active inlet valve
• Setable flow range: Setpoints 0.001 - 5 ml/min, in 0.001 ml/min increments
• Flow range 1 - 5.0 ml/min
• Flow precision: < 0.3 % RSD (typically 0.15 %), based on retention time, at 1 ml/min
• Pressure: Operating range 0 400 bar (0 - 5880 psi) up to 5 ml/min
• Pressure pulsation: < 2 %amplitude (typically < 1 %), at 1 ml/min isopropanol, at all pressures > 1 MPa
• Compressibility compensation: User-selectable, based on mobile phase compressibility
• Recommended pH range: 0 - 12.5, solvents with pH < 2.3 should not contain acids which attack stainless steel
• Gradient formation: High-pressure binary mixing, delay volume 180 - 480 μl without mixer, 600 - 900 μl with mixer, dependent on back pressure
• Composition range 1- 99 % or 5 μl/min per channel, whatever is greater
• Composition precision < 0.2 % SD, at 0.1 and 1 ml/min
• Control and data evaluation Agilent ChemStation for LC Control and data evaluation

Can be sold as an individual component or as part of a complete stack

Specifications:

• Hydraulic system: Two dual piston in series pumps with proprietary servo-controlled variable stroke drive, floating piston design and active inlet valve
• Setable flow range: Setpoints 0.001 - 5 ml/min, in 0.001 ml/min increments
• Flow range 1 - 5.0 ml/min
• Flow precision: < 0.3 % RSD (typically 0.15 %), based on retention time, at 1 ml/min
• Pressure: Operating range 0 400 bar (0 - 5880 psi) up to 5 ml/min
• Pressure pulsation: < 2 %amplitude (typically < 1 %), at 1 ml/min isopropanol, at all pressures > 1 MPa
• Compressibility compensation: User-selectable, based on mobile phase compressibility
• Recommended pH range: 0 - 12.5, solvents with pH < 2.3 should not contain acids which attack stainless steel
• Gradient formation: High-pressure binary mixing, delay volume 180 - 480 μl without mixer, 600 - 900 μl with mixer, dependent on back pressure
• Composition range 1- 99 % or 5 μl/min per channel, whatever is greater
• Composition precision < 0.2 % SD, at 0.1 and 1 ml/min
• Control and data evaluation Agilent ChemStation for LC Control and data evaluation

Can be sold as an individual component or as part of a complete stack

Specifications:

• Hydraulic system: Two dual piston in series, with proprietary servo-controlled variable stroke drive, floating piston, active inlet valve, solvent selection valve and electronic flow control for flow rates up to 100 µl/min
• Settable column flow Range:
  • – 20 µl/min
  • – 100 µl/min (with the extended flow range kit)
  • – 2.5 µl/min (with the electronic flow control bypassed)
• Recommended column flow range:
  • – 20 µl/min
  • 10 – 100 µl/min (with extended flow range kit)
  • – 2.5 ml/min (with the electronic flow sensor bypassed)
• Column flow precision: < 0.7 % RSD or 0.03 % SD (typically 0.4 % RSD or 0.02 % SD), at 10 µl/min and 50 µl/min column flow (based on RT, default setting)
• Optimum composition Range: 1 to 99% or 5 µl/min per channel (primary flow), whatever is greater
• Composition precision: < 0.2 % SD, at 10 µl/min (20 µl flow sensor), 50 µl/min (100 µl flow sensor) and 1 ml/min (normal mode) default setting
• Delay volume:
  • Typically 3 µl from the electronic flow control to the pump outlet for flow rates up to 20 µl/min.
  • Typically 12 µl from the electronic flow control to the pump outlet for flow rates up to 100 µl.
  • for flow rates up to 100 µl/min and electronic flow control active:
  • primary flow path 180 - 480 µl without mixer, 600 - 900 µl with mixer (system pressure dependent)
  • Typically 180 to 480 µl (system pressure dependent) without mixer for flow rates up to 2.5 ml/min. (Mixer delay volume 420 µl)
• Pressure range: 20 to 400 bar (5880psi) system pressure
• Compressibility Compensation: User-selectable, based on mobile phase compressibility
• Recommended pH Range: 0 – 8.5, solvents with pH < 2.3 should not contain acids which attack stainless steel. Upper pH range is limited by fused silica capillaries.
• Control and data Evaluation: Agilent ChemStation for LC
• Analog output For pressure monitoring, 2 mV/bar, one output
• Communications: Controller-area network (CAN), GPIB, RS-232C, APG Remote: ready, start, stop and shut-down signals, LAN optional
• Safety and maintenance: Extensive diagnostics, error detection and display (through control module and Agilent ChemStation), leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas.
• GLP features: Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of seal wear and volume of pumped mobile phase with user-settable limits and feedback messages. Electronic records of maintenance and errors.
• Housing: All materials recyclable

The G1311A is an optimized design ensuring virtually pulse-free and stable solvent flow with dual floating pistions.  An inlet valve electronically activated and synchronized to piston stroke eliminates vapor formation with volatile solvents and is maintenance free.  Instrument comes equipped with four solvent inlets with built-in gradient control. 

Specifications:

• Configurable Flow Range: 0.001 – 10ml/min – in 0.001ml/min increments
• Flow Range: 0.2 – 10.0 ml/min
• Recommended pH Range: 1.0 – 12.5, solvents with pH > 2.3 should not contain acids which attack stainless steel
• Gradient Formation: Low pressure quaternary mixing/gradient capability using proprietary high-speed proportioning valve. Delay volume 800-1100µl, depending on back pressure