Used Lab Equipment

Includes Installation and One Year Warranty (Preventative Maintenance at 6 months)

Method Development and Training also Available

Includes:

• AB Sciex API 3200 Mass Spectrometer LC/MS/MS
• Windows 7 Computer loaded w/ Analyst Software 1.5
• Turbo V-Spray ESI
• Vacuum pump
• Shimadzu Prominence 20 UFLC  Shimadzu
• Shimadzu DGU-20A3 Degasser
• (2)Shimadzu LC_20AD Liquid Chromatograph
• Shimadzu CTO Column Oven
• Shimadzu CBM-20A Communication Module
• CTC Autosampler
• Monitor – Mouse – Keyboard
• Manuals

The API 3200 LC/MS/MS system is a fully-integrated triple quadrupole mass spectrometer built using premier technology that combines sensitivity and selectivity with ruggedness and reliability, all in an affordable, compact package

• Innovative Turbo V ion source efficiently ionizes compounds over a wide range of flow rates, virtually eliminating cross-contamination, even with large sample loads
• Patented LINAC collision cell technology delivers superior MS/MS performance allowing faster scan times without compromising sensitivity or mass spectral quality
• Simplifies cross-platform methods transfer
• Gives meaningful results from every experiment

Specifications:

• Detector type: Pulse Counting CEM
• Dynamic Range: 5 orders of magnitude
• Ionization Sources: TurboIonSpray, APCI, DuoSpray, PhotoSpray
• Mass Accuracy / Stability: 0.1 Da over 8 hours and 0.15 Da over 24 hours
• Mass Range: 5-1,700 (Quad); 50-1,700 (LIT)
• Polarity Switching Time: 700 ms
• Scan Speed (Quad): 24,000 Da/sec
• Scan Types: Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM, EMS, EPI, ER, MS3, TripleTrap

Includes 1 year Service Contract, Installation, and a PM at 6 months

Method Development and Training also Available

Includes:

• AB Sciex API4000 LC/MS/MS
• Enhanced high performance triple quadrupole mass spectrometer system
• Line transformers
• Turbo V Ion Source (with APCI and ESI probes)
• Roughing Pump
• Windows 7 Computer loaded w/ Analyst Software 1.6
• Cart
• Shimadzu Prominence 20 UFLC  Shimadzu
  • Shimadzu DGU-20A3 Degasser
  • (2)Shimadzu LC_20AD Liquid Chromatograph
  • Shimadzu CTO Column Oven
  • Shimadzu CBM-20A Communication Module
• CTC Autosampler
• Monitor – Mouse – Keyboard
• Cables and Manuals

Specifications:

• Detector type: Pulse Counting CEM
• Dynamic Range: 5 orders of magnitude
• Ionization Sources: ESI, APCI
• Mass Accuracy / Stability: 0.1 Da over 8 hours, 0.15 Da over 24 hours
• Mass Range: 5-3,000
• Polarity Switching Time: 700 ms
• Scan Speed (Quad): 24,000 Da/sec
• Scan Types: Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM
• Sensitivity MRM Mode: 200 fg Reserpine on column: S/N > 1,200, C.V. < 5%

Includes:

• AB Sciex API4000 LC/MS/MS
• Enhanced high performance triple quadrupole mass spectrometer system
• Line transformers
• Turbo V Ion Source (with HESI probes)
• Roughing Pump
• Windows 7 Computer loaded w/ Analyst Software 1.6
• Cart
• Optional Shimadzu Front End
• Monitor – Mouse – Keyboard
• Cables and Manuals

Specifications:

• Detector type: Pulse Counting CEM
• Dynamic Range: 5 orders of magnitude
• Ionization Sources: ESI, APCI
• Mass Accuracy / Stability: 0.1 Da over 8 hours, 0.15 Da over 24 hours
• Mass Range: 5-3,000
• Polarity Switching Time: 700 ms
• Scan Speed (Quad): 24,000 Da/sec
• Scan Types: Q1 MS, Q3 MS, Product Ion, Precursor Ion, Neutral Loss or Gain, MRM
• Sensitivity MRM Mode: 200 fg Reserpine on column: S/N > 1,200, C.V. < 5%

Optional Shimadzu UFLC System Components:

• SIL-20AC
• LC-20AB
• CTO-20AC
• CBM-20A
• DGU-20A₅

This LCMS brings you the best in quantitative sensitivity and robustness to expand upon the experiments going beyond MRM, and give you substantial improvements in data quality.

Includes:

• AB Sciex 4500 LC/MS/MS
• Shimadzu Prominence 20 UFLC  
• Shimadzu DGU-20A3 Degasser
• (2)Shimadzu LC_20AD Liquid Chromatograph
• Shimadzu CTO-20AC Column Oven
• Shimadzu SIL-20AC UFLC
• Windows 7 Computer Loaded with Analyst 1.6 Software       

Specifications:

• Sensitivity MRM: mode Reserpine 200 fg on column S/N > 2000  C.V. < 5%
• Maximum scan speed: 12,000 Da/sec
• Polarity switching time: 50 msec, in MRM and scheduled MRM (sMRM) modes
• Minimum MRM dwell time: 1 msec
• Mass range (m/z): 5-2000
• Cross talk for reserpine 609/195: <0.5% cross talk detectable with 2 msec dwell time and 3 msec inter-MRM pause time
• Triple quadrupole mass stability: 0.1 Da over 24 hours
• Scan types: Full scan MS and selected ion MS for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, multiple reaction monitoring (MRM), and scheduled MRM (sMRM)
• Detector type: AcQuRate Pulse Counting CEM
• Dynamic range: 4 orders of magnitude
• Ionization sources: Turbo V source housing with TurboIonSpray probe or APCI probe.
• Maximum temperature: 750ºC
• Flow rate compatibility: 5 μL/minute to 3 mL/minute
• Power: 208V 50/60Hz AB Sciex 4500, 208V Vacuum Pump, 208V Peak N2 Generator, 115V Shimadzu UPLC
• Dimensions: 37" x 33" x 55" Sciex 4500
• Weight: 250lbs

Includes One Year Service Contract, PM at 6 Months, and Installation

The AB SCIEX QTRAP 5500 System is a high sensitivity, bench top hybrid triple quadrupole-Linear Accelerator trap mass spectrometer designed for LC/MS/MS analyses. This instrument provides an uncompromised combination of Linear Accelerator trap and triple quadrupole functionality, uniquely allowing both  qualitative and quantitative analyses to be carried out in a single experiment.

Includes:

• AB Sciex 5500 Qtrap
• Shimadzu Prominence 20 UFLC  Shimadzu
  • Shimadzu DGU-20A3 Degasser
  • (2)Shimadzu LC_20AD Liquid Chromatograph
  • Shimadzu CTO Column Oven
  • Shimadzu CBM-20A Communication Module
  • CTC Autosampler
  • Computer Loaded with Analyst 1.6 Software       

Specifications

• Sensitivity MRM mode Reserpine: 50 fg on column S/N > 2000
• V.: < 5%
• Triple quad scan speed: 12,000 Da/sec
• Linear ion trap scan speed: 20,000 Da/sec
• Polarity switching time: 50 msec
• Minimum MRM Dwell Time: 1 msec
• Triple quad mass range (m/z): 5-1250
• Linear ion trap mass range (m/z): 50-1000
• Cross talk for Reserpine 609/195: No significant cross talk detectable with 1 msec dwell time and 3 msec inter-MRM pause time
• Triple quadrupole mass stability: 0.1 Da over 24 hours
• Scan types: Full scan MS and selected ion for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, multiple reaction monitoring (MRM), enhanced MS scan, enhanced product ion scan, enhanced resolution scan, MS  scan, MRM3 scan, and TripleTrap™ scan modes

Features:

• <400 uL internal volume
• Plugs into LC-20A/LC-30A series pump for power and control
• New material (Systec AF) allows high gas permeability
• Peak efficiency in under 1 minute
• Additional channel provided for autosampler rinse solution

A proprietary band function enables obtaining accurate fractions even when the peak elution time varies, by catching the target component according to variations in the chromatogram. If connected to workstation software, fractions can be simulated on screen to determine whether or not the fraction program is appropriate.

Details:

• Small and Large Volume Collection Capacity
• The FRC-10A collects both analytical and preparative fractions. The standard configuration has a 144 5mL vial capacity. The large volume kit can be added for large volume collection.
• Precise Peltier Temperature Control
• For automated collection of thermally-labile fractions, Peltier temperature control keeps temperatures stable within a 4-70º C range.
• Simplified Graphical Parameter Entry
• Set up fractionation parameters graphically from the SCL-10AVP System Controller. Eliminate the guesswork of determining slope and level values.
• Fraction Collection Flexibility
• Tailor the collection to your application requirements.  Choose from collection criteria such as volume, threshold, and peak purity. A precise peak division feature ensures high purity fractions. The FRC-10A automatically adjusts for retention time shifts, so that only the peak of interest is collected. Our slope-override capability enables continued collection, even when the detector signal is off-scale.

Specifications:

• Drive System and Fraction Collection Methods: Arm-Movement X-Y System
• Select either solenoid valve or direct through nozzle
• Fraction Modes: Manual or programmed fraction collection by combining 14 types of parameters, such as slope, level, and band
• Number of Fractions: 16 to 144
• Collection Tubes: Glass: 3.5, 5, 20, 32, or 50 mL, or user supplied
• Polypropylene: 4.5, 5, 25, or 50 mL, or user supplied

The Shimadzu triple-quad GCMS-TQ8050 NX is capable of performing unprecedented quantitative GC-MS/MS analyses of ultra-trace amounts, down to the femtogram level. Equipped with a new, highly efficient detector and three forms of noise-reduction technologies, the GCMS-TQ8050 NX has never been more important in industries such as food safety, cannabis testing, forensics, and more.

System includes Shimadzu GCMS-TQ8050 NX EI 115V with rough pump, AOC-20i, and GC-2030

Shimadzu's Cannabis and Hemp Testing Solutions cover a broad range of applications, from accurate potency testing and terpene profiling to contaminate testing for pesticides, residual solvents, heavy metals, and mycotoxins/aflatoxins. We supply the instruments, methods and experience necessary to get you up and running quickly. Shimadzu scientific instruments have been applied to natural products, food sciences, pharmaceuticals and environmental testing for decades. Whether you are a chromatography expert or a novice, our platforms and training ensure that your laboratory will generate quality results from a wide variety of cannabis samples. Our easy to use platforms save you time and money, maximizing the profits of your laboratory. Shimadzu can help you with your QA/QC testing, peak harvesting analysis and cannabis research.

System Includes:
Shimadzu Hemp Analyzer - Prominence 2030-C HPLC with Computer, Computer Interface, Column, Hemp Analyzer Solution.

The LC-20AT possesses a high level of stability while maintaining high performance during routine use. The ability to remove pulsations has been improved by modifying the pump-head structure and the flow line.

Features:

• Enhanced Solvent Delivery Specifications: Flow-rate accuracy and precision in the micro-flow rate region have been improved with the addition of a new type of check valve and modifications to the solvent delivery control method. Non-polar organic solvents such as hexane can be delivered stably.
• Improved Durability: New and improved plunger seal materials ensure robust, long-lasting performance. A sapphire plunger optimized according to its crystal structure and a precise plunger-holding mechanism help increase the service life of plunger seals and enable stable solvent delivery over long periods.
• Space-saving Designs: An optional low pressure gradient valve (LC-20AD/20AT), CBM-20Alite system controller, and a seal wash pump (LC-20AD) can now be installed inside the solvent delivery unit, enabling 4-solvent gradient elution in a compact space. The LC-20AB high-pressure binary gradient pump delivers the performance of two LC-20AD pumps in one compact unit.

Specifications:

• Solvent delivery method: Series-type double plunger
• Plunger capacity: Primary side: 47µL, Secondary side: 23µL
• Maximum discharge pressure: 40MPa
• Flow-rate setting range: 0.001 to 10.000 mL/min.
• Flow-rate accuracy: No more than 2% or 2µL/min., whichever is greater (0.01 to 5 mL/min.)
• Flow-rate precision: No more than 0.06% RSD or 0.02 min SD, whichever is greater
• Pulsation: 0.3 MPa (for water at 1.0 mL/min. and 7MPa)
• Constant-pressure solvent delivery: Supported
• Plunger rinsing mechanism: Manual rinsing or automatic rinsing using optional product
• Safety measures: Liquid-leakage sensor, high-pressure/low-pressure limits
• Operating temperature range: 4oC to 35oC
• Dimensions, weight: 260 (W) x 140 (H) x 420 (D) mm, 11 kg
• Power requirements: 100 VAC, 150 VA, 50/60 Hz 
• Gradient type: High-pressure mixing
• Number of mixed solvents: 2 or 3
• Mixing concentration accuracy: 0.5% max. (LC-20AD), 1.0% max. (LC-20AT)

Features:

• <400 uL internal volume
• Plugs into LC-20A/LC-30A series pump for power and control
• New material (Systec AF) allows high gas permeability
• Peak efficiency in under 1 minute
• Additional channel provided for autosampler rinse solution

Optional Computer Loaded w/ Clarity Software

Includes:

• Shimadzu DGU-20A3 Degasser
• (2)Shimadzu LC_20AD Liquid Chromatograph
• Shimadzu CTO Column Oven
• Shimadzu CBM-20A Communication Module
• SPD-20A Detector UV/vis Detector
• SIL-20A Auto Sampler

 Includes:

• Shimadzu DGU-20A5R Degasser
• CTO-20AC PROMINENCE COLUMN OVEN
• CBM-20A PROMINENCE COLUMN MODULE
• 2 LC-20ADXR PROMIENCE LIQUID Chromatography 

Specifications:

The LC-20ADXR offers an extended pressure tolerance over traditional HPLC (up to 66 mPa) while maintaining stable solvent delivery with reliable performance across an extensive analytical flow rate range. This pump also includes automatic rinsing to ensure improved plunger seal life under high-pressure delivery conditions.

The CTO-20AC can heat and cool the column compartment, utilizing a Peltier cooling device to provide sub-ambient conditions. Temperature control is regulated over a wide range, from 10ºC below room temperature to 85ºC, for increased reproducibility and separation performance.

A stand-alone system controller designed for maximum flexibility. Up to twelve LC modules and two channels of analog data can be connected for acquisition.

The chilled rackchanger unit exchanges the microplates on autosampler racks to enable samples to be continuously analyzed. 12 plates can be mounted inside the main unit and stored under refrigerated conditions.

Specifications:

• Method: Variable sample injection volume and total volume direct injection
• Injection Volume Range: 0.1 µL to 100 µL (0.1 µL to 2000 µL with option)
• Number of Samples Processed:
  • 175 (1-mL vials), 105 (1.5-mL vials), 50 (4-mL vials),
  • 192 (two 96-well MTP/DWP), 768 (two 384-well MTP/DWP)
  • *Twelve 96-well MTP/DWP in the rackchanger
• Injection Volume Precision: Max RSD 0.3 % (under specified conditions)
• Cross-Contamination: Max 0.005 % (naphthalene and chlorhexidine)
• Needle Rinsing: Freely settable, before or after sample injection

To be used with a Shimadzu 10 HPLC System

Specifications:

• Sample injection system: Total sample injection, variable sample injection system (zero sample loss during injection)
• Settable range of injection volumes: to 100 µL (standard), or 1 to 2000 µL (option) (0.1µL steps from 0.1 to 0.9µL, and 1µL steps from 1 to 2000 µL)
• Sample processing capability:
  • With 1-mL vials: 350
  • With 1.5-mL vials: 140
  • with 4-mL vials:100
  • With micro plates: 4 (96 wells: 284, 284 wells: 1536)
  • with deep well plates: 4 (96 wells: 284, 284 wells: 1536)
• Injection volume repeatability: RSD: 0.3% max. (at 10µL injection)
• Cross contamination: 01% max. (for analysis of naphthalene)
• Injection  volume accuracy:Less than +/- 1% (50µL)
• Injection volume accuracy correction: Possible
• of injections: 1-99 times per sample
• Setting of analysis time: .01– 9999.9 (0.1 minute increments to 999.99 min., 0.1 minutes increments over 1000 min.)
• Number of steps for injection conditions: Max 102 steps
• Sample suction speed: 1-15 µL/sec (0.1µL/s step for 0.1-0.9 µL/sec., 1µL/s step for over1 µL/sec.)
• Rinsing liquid suction speed: 1-35 µL/sec/ (1µL/s step)
• Maximum pressure: 20.0 Mpa (standard pippings of sample flowpath is PEEK)

Sample cooler (SIL-HTc only)

• Method: Direct cooling method (at a setting of 4 deg. C, room temperature must be less than 30 deg. Cand humidity less than 70%)
• Temperature setting range: 4 to 40 deg. (cooling down to 4 deg. C for room temperature up to 30 deg. C and humidity to 70%)
• Operating ambient temperature range:4 to 35 deg. C